Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization
Correspondence: danielrivaldi@gmail.com.
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| Otros Autores: | , , , , |
| Formato: | article |
| Lenguaje: | inglés |
| Publicado: |
2022
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| Acceso en línea: | https://doi.org/10.3390/su141811386 http://hdl.handle.net/20.500.14066/4741 |
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Sin Etiquetas, Sea el primero en etiquetar este registro!
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| _version_ | 1870612064882393088 |
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| author | Velázquez Figueredo, María Edelira |
| author2 | Ferreiro Balbuena, Omayra Beatriz Menezes, Diego Batista Corrales Ureña, Yendry Vega Baudrit, José Roberto Rivaldi Chávez, Juan Daniel |
| author2_role | author author author author author |
| author_browse | Corrales Ureña, Yendry Ferreiro Balbuena, Omayra Beatriz Menezes, Diego Batista Rivaldi Chávez, Juan Daniel Vega Baudrit, José Roberto Velázquez Figueredo, María Edelira |
| author_facet | Velázquez Figueredo, María Edelira Ferreiro Balbuena, Omayra Beatriz Menezes, Diego Batista Corrales Ureña, Yendry Vega Baudrit, José Roberto Rivaldi Chávez, Juan Daniel |
| author_role | author |
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| bitstream.url.fl_str_mv | http://repositorio.conacyt.gov.py/bitstream/20.500.14066/4741/3/license.txt http://repositorio.conacyt.gov.py/bitstream/20.500.14066/4741/1/Nanocellulose%20extracted%20from%20Paraguayan%20residual%20agro-industrial%20biomass%3a%20extraction%20process%2c%20physicochemical%20and%20morphological%20characterization.pdf http://repositorio.conacyt.gov.py/bitstream/20.500.14066/4741/2/license_rdf http://repositorio.conacyt.gov.py/bitstream/20.500.14066/4741/4/Nanocellulose%20extracted%20from%20Paraguayan%20residual%20agro-industrial%20biomass%20extraction%20process%2c%20physicochemical%20and%20morphological%20characterization.jpg http://repositorio.conacyt.gov.py/bitstream/20.500.14066/4741/5/Nanocellulose%20extracted%20from%20Paraguayan%20residual%20agro-industrial%20biomass%3a%20extraction%20process%2c%20physicochemical%20and%20morphological%20characterization.pdf.txt |
| dc.contributor.other.es.fl_str_mv | Universidad Americana/INCADE S.A.E |
| dc.creator.none.fl_str_mv | Velázquez Figueredo, María Edelira Ferreiro Balbuena, Omayra Beatriz Menezes, Diego Batista Corrales Ureña, Yendry Vega Baudrit, José Roberto Rivaldi Chávez, Juan Daniel |
| dc.date.accessioned.none.fl_str_mv | 2026-01-27T15:20:51Z |
| dc.date.available.none.fl_str_mv | 2026-01-27T15:20:51Z |
| dc.date.issued.none.fl_str_mv | 2022-09-10 |
| dc.format.extent.es.fl_str_mv | 15 páginas |
| dc.identifier.citation.en.fl_str_mv | Velázquez, M. E., Ferreiro, O. B., Menezes, D. B., Corrales-Ureña, Y., Vega-Baudrit, J. R., & Rivaldi, J. D. (2022). Nanocellulose Extracted from Paraguayan Residual Agro-Industrial Biomass: Extraction Process, Physicochemical and Morphological Characterization. Sustainability, 14(18), Artículo 11386. https://doi.org/10.3390/su141811386 |
| dc.identifier.doi.es.fl_str_mv | 10.3390/su141811386 |
| dc.identifier.issn.es.fl_str_mv | 2071-1050 |
| dc.identifier.other.es.fl_str_mv | https://doi.org/10.3390/su141811386 |
| dc.identifier.uri.none.fl_str_mv | http://hdl.handle.net/20.500.14066/4741 |
| dc.language.iso.es.fl_str_mv | eng |
| dc.publisher.es.fl_str_mv | Multidisciplinary Digital Publishing Institute |
| dc.relation.projectCONACYT.es.fl_str_mv | PINV18-128 |
| dc.rights.*.fl_str_mv | Atribución/Reconocimiento 4.0 Internacional |
| dc.rights.accessRights.es.fl_str_mv | info:eu-repo/semantics/openAccess |
| dc.rights.uri.*.fl_str_mv | http://creativecommons.org/licenses/by/4.0/ |
| dc.subject.classification.es.fl_str_mv | 6. Producción y tecnología industrial 6.2. Productos industriales y sus procesos de fabricación |
| dc.subject.ocde.es.fl_str_mv | 2. Ingeniería y Tecnología 2.3. Otras ingenierías (tales como ingeniería química, aeronáutica y aeroespacial, mecánica, metalúrgica, de los materiales y sus correspondientes subdivisiones especializadas; productos forestales; ciencias aplicadas, como geodesia, química industrial, etc.; ciencia y tecnología de los alimentos; tecnologías especializadas o áreas interdisciplinares, por ejemplo, análisis de sistemas, metalurgia, minería) |
| dc.subject.other.es.fl_str_mv | Acid hydrolysis Nanocellulose Residual biomass Soybean hulls Sugarcane bagasse |
| dc.title.es.fl_str_mv | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization |
| dc.type.es.fl_str_mv | info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
| description | Correspondence: danielrivaldi@gmail.com. |
| eu_rights_str_mv | openAccess |
| format | article |
| id | CONACYT_0b4db5c38ac090d32afcb07f78a32c06 |
| identifier_str_mv | Velázquez, M. E., Ferreiro, O. B., Menezes, D. B., Corrales-Ureña, Y., Vega-Baudrit, J. R., & Rivaldi, J. D. (2022). Nanocellulose Extracted from Paraguayan Residual Agro-Industrial Biomass: Extraction Process, Physicochemical and Morphological Characterization. Sustainability, 14(18), Artículo 11386. https://doi.org/10.3390/su141811386 2071-1050 10.3390/su141811386 |
| language | eng |
| network_acronym_str | CONACYT |
| network_name_str | Repositorio Institucional CONACYT |
| oai_identifier_str | oai:repositorio.conacyt.gov.py:20.500.14066/4741 |
| publishDate | 2022 |
| publishDateSort | 2022 |
| repository.mail.fl_str_mv | repositorio.institucional@conacyt.gov.py |
| repository.name.fl_str_mv | Repositorio Institucional CONACYT |
| repository_id_str | |
| rights_invalid_str_mv | Atribución/Reconocimiento 4.0 Internacional http://creativecommons.org/licenses/by/4.0/ |
| spelling | 960cfdbf-c7ca-4313-9c7f-74f971d81a4d60012726000000-0001-8449-1297f61ac03d-d713-4f31-9129-1f36f41951a7600c7601f1a-bc30-4cc4-a9a2-cef32dcd12ca6008261babd-7bdf-41d2-92d8-bf180b5272ed600955600Universidad Americana/INCADE S.A.E2026-01-27T15:20:51Z2026-01-27T15:20:51Z2022-09-10Velázquez, M. E., Ferreiro, O. B., Menezes, D. B., Corrales-Ureña, Y., Vega-Baudrit, J. R., & Rivaldi, J. D. (2022). Nanocellulose Extracted from Paraguayan Residual Agro-Industrial Biomass: Extraction Process, Physicochemical and Morphological Characterization. Sustainability, 14(18), Artículo 11386. https://doi.org/10.3390/su1418113862071-1050https://doi.org/10.3390/su141811386http://hdl.handle.net/20.500.14066/474110.3390/su141811386Correspondence: danielrivaldi@gmail.com.This article belongs to the Special Issue Biomass Treatment Techniques and Sustainable Utilization of Residues.Residual biomasses from agro-industries in Paraguay, including soybean hulls (SBHs) and sugarcane bagasse (SCB), were studied as a source for nanocellulose extraction for the first time. For that purpose, both biomasses were delignified in a semi-pilot stainless-steel reactor, and the cellulose pulp was subjected to a bleaching process with NaClO (2.5%, w/v). The nanocellulose (CNC) was obtained after two-step acid hydrolysis. Firstly, the bleached cellulose was hydrolyzed with HCl (17%, w/w) for two hours at 60 °C to obtain microcrystals by removing most of the amorphous fraction. The celluloses were then treated with H2SO4 (65%, w/w) at 45 °C for 45 min to obtain nanocellulose. Physicochemical and morphological properties were analyzed using attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), atomic force microscopy (AFM), and X-ray diffraction analysis (XRD). The SBHs nanocellulose had a whisker-like form with a 230 ± 42 nm diameter and a 12 ± 2 nm height, and the SCB nanocellulose had a fibril-like form with a 103 ± 30 nm diameter and a height of 6 ± 3 nm. The nanocellulose from SBHs and SCB had good thermal stability as its degradation temperature started at 250 °C. Furthermore, the nanocellulose obtained was negatively charged and formed stable dispersion in water at 0.1 mg/mL concentration and a pH of around 6.5.Consejo Nacional de Ciencia y TecnologíaPrograma Paraguayo para el Desarrollo de la Ciencia y Tecnología. Proyectos de investigación y desarrollo15 páginasengMultidisciplinary Digital Publishing InstituteAtribución/Reconocimiento 4.0 Internacionalhttp://creativecommons.org/licenses/by/4.0/info:eu-repo/semantics/openAccess© 2022 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https:// creativecommons.org/licenses/by/ 4.0/).6. Producción y tecnología industrial6.2. Productos industriales y sus procesos de fabricaciónAcid hydrolysisNanocelluloseResidual biomassSoybean hullsSugarcane bagasse2. Ingeniería y Tecnología2.3. Otras ingenierías (tales como ingeniería química, aeronáutica y aeroespacial, mecánica, metalúrgica, de los materiales y sus correspondientes subdivisiones especializadas; productos forestales; ciencias aplicadas, como geodesia, química industrial, etc.; ciencia y tecnología de los alimentos; tecnologías especializadas o áreas interdisciplinares, por ejemplo, análisis de sistemas, metalurgia, minería)Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterizationinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersion18SustainabilityPINV18-12814Velázquez Figueredo, María EdeliraFerreiro Balbuena, Omayra BeatrizMenezes, Diego BatistaCorrales Ureña, YendryVega Baudrit, José RobertoRivaldi Chávez, Juan DanielLICENSElicense.txtlicense.txttext/plain; charset=utf-81698http://repositorio.conacyt.gov.py/bitstream/20.500.14066/4741/3/license.txt858b22fda432bd774e469302988c1974MD53ORIGINALNanocellulose extracted from Paraguayan residual agro-industrial biomass: extraction process, physicochemical and morphological characterization.pdfNanocellulose extracted from Paraguayan residual agro-industrial biomass: extraction process, physicochemical and morphological characterization.pdfArtículo científicoapplication/pdf2563835http://repositorio.conacyt.gov.py/bitstream/20.500.14066/4741/1/Nanocellulose%20extracted%20from%20Paraguayan%20residual%20agro-industrial%20biomass%3a%20extraction%20process%2c%20physicochemical%20and%20morphological%20characterization.pdf338228cbc9d02f7023316f5cff057cfcMD51CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; 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| spellingShingle | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization Velázquez Figueredo, María Edelira 6. Producción y tecnología industrial 6.2. Productos industriales y sus procesos de fabricación Acid hydrolysis Nanocellulose Residual biomass Soybean hulls Sugarcane bagasse 2. Ingeniería y Tecnología 2.3. Otras ingenierías (tales como ingeniería química, aeronáutica y aeroespacial, mecánica, metalúrgica, de los materiales y sus correspondientes subdivisiones especializadas; productos forestales; ciencias aplicadas, como geodesia, química industrial, etc.; ciencia y tecnología de los alimentos; tecnologías especializadas o áreas interdisciplinares, por ejemplo, análisis de sistemas, metalurgia, minería) |
| status_str | publishedVersion |
| title | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization |
| title_full | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization |
| title_fullStr | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization |
| title_full_unstemmed | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization |
| title_short | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization |
| title_sort | Nanocellulose extracted from Paraguayan residual agro-industrial biomass : extraction process, physicochemical and morphological characterization |
| topic | 6. Producción y tecnología industrial 6.2. Productos industriales y sus procesos de fabricación Acid hydrolysis Nanocellulose Residual biomass Soybean hulls Sugarcane bagasse 2. Ingeniería y Tecnología 2.3. Otras ingenierías (tales como ingeniería química, aeronáutica y aeroespacial, mecánica, metalúrgica, de los materiales y sus correspondientes subdivisiones especializadas; productos forestales; ciencias aplicadas, como geodesia, química industrial, etc.; ciencia y tecnología de los alimentos; tecnologías especializadas o áreas interdisciplinares, por ejemplo, análisis de sistemas, metalurgia, minería) |
| url | https://doi.org/10.3390/su141811386 http://hdl.handle.net/20.500.14066/4741 |