Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique

The present investigation is related to the synthesis of polymeric membranes with piezoelectric characteristics, using the vinylidene polyfluoride (PVDF) material, which is a thermoplastic semicrystalline polymer; the membranes will be made up of micro and nano piezoelectric fibers of this material,...

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সংরক্ষণ করুন:
গ্রন্থ-পঞ্জীর বিবরন
প্রধান লেখক: de Obaldia, Elida (author)
অন্যান্য লেখক: Miranda, Adrián (author), Boya, Aurelio (author)
বিন্যাস: article
ভাষা:স্প্যানিশ
প্রকাশিত: 2021
অনলাইন ব্যবহার করুন:https://revistas.utp.ac.pa/index.php/id-tecnologico/article/view/2989
https://ridda2.utp.ac.pa/handle/123456789/13122
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author de Obaldia, Elida
author2 Miranda, Adrián
Boya, Aurelio
author2_role author
author
author_browse Boya, Aurelio
Miranda, Adrián
de Obaldia, Elida
author_facet de Obaldia, Elida
Miranda, Adrián
Boya, Aurelio
author_role author
collection Repositorio Institucional de documento digitales de acceso abierto de la UTP
dc.creator.none.fl_str_mv de Obaldia, Elida
Miranda, Adrián
Boya, Aurelio
dc.date.none.fl_str_mv 2021-03-01
2021-05-12T23:22:03Z
2021-06-01T05:47:43Z
2021-05-12T23:22:03Z
2021-06-01T05:47:43Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://revistas.utp.ac.pa/index.php/id-tecnologico/article/view/2989
10.33412/idt.v17.1.2989
https://ridda2.utp.ac.pa/handle/123456789/13122
dc.language.none.fl_str_mv spa
dc.publisher.none.fl_str_mv Universidad Tecnológica de Panamá
dc.relation.none.fl_str_mv https://revistas.utp.ac.pa/index.php/id-tecnologico/article/view/2989/3686
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/4.0/
dc.source.none.fl_str_mv 2219-6714
1680-8894
I+D Tecnológico; Vol. 17 Núm. 1 (2021): Revista de I+D Tecnológico
reponame:Repositorio Institucional de documento digitales de acceso abierto de la UTP
instname:Universidad Tecnológica de Panamá
instacron:U Tecnológica de Panamá
dc.title.none.fl_str_mv Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
Síntesis y caracterización de membranas piezoeléctricas en base al polímero polifluoruro de vinilideno, utilizando la técnica de electrospinning
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
description The present investigation is related to the synthesis of polymeric membranes with piezoelectric characteristics, using the vinylidene polyfluoride (PVDF) material, which is a thermoplastic semicrystalline polymer; the membranes will be made up of micro and nano piezoelectric fibers of this material, which were manufactured using the Electrospinning technique, the separation distance of 4.5 cm, 8.5 cm, 11.5 cm from the needle The hypodermic ones referring to the collecting cylinder were the one used to collect the samples. The hypothesis of manufacturing process parameters related to the diameter of the micro and nanofibers of the piezoelectric material PVDF with its rotational structure Beta (β) was tested. The following techniques were performed: XRD, where the dispersion of the samples were 18.3o, 19.9o, 20.6o, is related to the internal rotational structure α and β, for the SEM the approximate diameter of 100 to 250 nm was obtained of the micro and nano fibers of the PVDF, two protocols were applied to the FTIR for the analysis of the spectra, one of them with bibliographic reference and the other with the frequency changes shown with the baseline and modified the nano fibrous membranes of the PVDF , in Raman the spectrum from 800 to 840 cm-1 shows the changes in its internal rotational structure of the modified and unmodified PVDF by bibliographic reference is observed with a qualitative analysis.
eu_rights_str_mv openAccess
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spelling Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning techniqueSíntesis y caracterización de membranas piezoeléctricas en base al polímero polifluoruro de vinilideno, utilizando la técnica de electrospinningde Obaldia, ElidaMiranda, AdriánBoya, AurelioThe present investigation is related to the synthesis of polymeric membranes with piezoelectric characteristics, using the vinylidene polyfluoride (PVDF) material, which is a thermoplastic semicrystalline polymer; the membranes will be made up of micro and nano piezoelectric fibers of this material, which were manufactured using the Electrospinning technique, the separation distance of 4.5 cm, 8.5 cm, 11.5 cm from the needle The hypodermic ones referring to the collecting cylinder were the one used to collect the samples. The hypothesis of manufacturing process parameters related to the diameter of the micro and nanofibers of the piezoelectric material PVDF with its rotational structure Beta (β) was tested. The following techniques were performed: XRD, where the dispersion of the samples were 18.3o, 19.9o, 20.6o, is related to the internal rotational structure α and β, for the SEM the approximate diameter of 100 to 250 nm was obtained of the micro and nano fibers of the PVDF, two protocols were applied to the FTIR for the analysis of the spectra, one of them with bibliographic reference and the other with the frequency changes shown with the baseline and modified the nano fibrous membranes of the PVDF , in Raman the spectrum from 800 to 840 cm-1 shows the changes in its internal rotational structure of the modified and unmodified PVDF by bibliographic reference is observed with a qualitative analysis.La presente investigación está relacionada con la síntesis de membranas poliméricas con características piezoeléctricas, utilizando el material polifloururo de vinilideno (PVDF), el cual es un polímero semicristalino termoplástico. Las membranas estarán conformadas por micro y nanofibras piezoeléctricas de este material, las cuales fueron fabricadas a través de la técnica de Electrospinning, en la misma se utilizaron distancias de separación de 4.5 cm, 8.5 cm, 11.5 cm entre la aguja hipodérmica y el cilindro electrizado colector de muestras.  Se sometió a prueba la hipótesis del efecto de los parámetros del proceso de fabricación de las membranas, sobre el diámetro de la micros y nanofibras del material piezoeléctrico (PVDF) y en la estructura rotacional de la fase piezoeléctrica Beta (β). Se realizaron las siguientes técnicas de caracterización. XRD, donde la  dispersión  de las muestras  eran 18.3o, 19.9o, 20.6o, lo cual tienen relación con la estructura interna rotacional α y β; SEM, en la que se obtuvo el diámetro aproximado 100 a 250 nm  de las micro y nano fibras del (PVDF); FTIR, en la cual se aplicaron dos protocolos para el análisis de los espectros: una de ella con referencia bibliográfica y otra con los cambios de frecuencia que se muestra con la línea de base y modificado de las membranas nano fibrosas del PVDF. Espectroscopía Raman, con la que se determinó un espectro de 800 a 840 cm-1, lo cual muestra los cambios de la estructura interna rotacional del PVDF modificado y no modificado, indicado en referencias bibliográficas con un análisis cualitativo.Universidad Tecnológica de Panamá2021-03-012021-05-12T23:22:03Z2021-06-01T05:47:43Z2021-05-12T23:22:03Z2021-06-01T05:47:43Zinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://revistas.utp.ac.pa/index.php/id-tecnologico/article/view/298910.33412/idt.v17.1.2989https://ridda2.utp.ac.pa/handle/123456789/131222219-67141680-8894I+D Tecnológico; Vol. 17 Núm. 1 (2021): Revista de I+D Tecnológicoreponame:Repositorio Institucional de documento digitales de acceso abierto de la UTPinstname:Universidad Tecnológica de Panamáinstacron:U Tecnológica de Panamáspahttps://revistas.utp.ac.pa/index.php/id-tecnologico/article/view/2989/3686info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/4.0/oai:ridda2.utp.ac.pa:123456789/131222021-06-01T05:47:43Z
spellingShingle Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
de Obaldia, Elida
status_str publishedVersion
title Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
title_full Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
title_fullStr Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
title_full_unstemmed Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
title_short Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
title_sort Synthesis and characterization of piezoelectric membranes in based on the olyvinylidene polymer, using electrospinning technique
url https://revistas.utp.ac.pa/index.php/id-tecnologico/article/view/2989
https://ridda2.utp.ac.pa/handle/123456789/13122